Title: 4'-Chloro-biphenyl-3-yl 2,2,2-trichloro-ethyl sulfate.
Authors: Li, Xueshu; Parkin, Sean; Duffel, Michael W; Robertson, Larry W; Lehmler, Hans-Joachim
Published In Acta Crystallogr Sect E Struct Rep Online, (2010 Aug 18)
Abstract: The title compound, C(14)H(10)Cl(4)O(4)S, is a 2,2,2-trichloro-ethyl-protected precursor of 4'-chloro-biphenyl-3-yl sulfate, a sulfuric acid ester of 4'-chloro-biphenyl-3-ol. The C(aromatic)-O and O-S bond lengths of the C(aromatic)-O-S unit are comparable to those in structurally analogous biphenyl-4-yl 2,2,2-trichloro-ethyl sulfates with no electro-negative chlorine substituent in the benzene ring with the sulfate ester group. The dihedral angle between the aromatic rings is 27.47 (6)°.
PubMed ID: 21588655
MeSH Terms: No MeSH terms associated with this publication