Skip Navigation

University of Iowa: Dataset Details, ID=doi: 10.6084/m9.figshare.8269931.v1.

Maintenance notice: We are currently addressing issues with broken links due to recent major website changes. We apologize for any inconvenience and appreciate your patience. Please contact for assistance.

Superfund Research Program

Airborne PCBs: Sources, Exposures, Toxicities, Remediation

Center Director: Keri C. Hornbuckle
Grant Number: P42ES013661
Funding Period: 2006-2025
View this project in the NIH Research Portfolio Online Reporting Tools (RePORT)

Program Links

Connect with the Grant Recipients

Visit the grantee's eNewsletter page Visit the grantee's eNewsletter page Visit the grantee's Twitter page

Title: Authentication of 5-bromo-3-chloro-1,2-dimethoxybenzene

Accession Number: doi: 10.6084/m9.figshare.8269931.v1.

Link to Dataset:

Repository: figshare

Data Type(s): Chemical & Chemical Biology

Summary: Authentication of 5-bromo-3-chloro-1,2-dimethoxybenzene by NMR and GC-MS. This compound was synthesized from 4-bromo-2-chloro-6-fluoroanisole via aromatic nucleophilic substitution in the presence of sodium methoxide and is a precursor for the preparation of 3,3'-dichloro-4,5-dimethoxy-biphenyl, a derivative of PCB 11 (3,3'-dichlorobiphenyl).

Publication(s) associated with this dataset:
  • Li X, Holland EB, Feng W, Zheng J, Dong Y, Pessah IN, Duffel MW, Robertson LW, Lehmler H. 2018. Authentication of synthetic environmental contaminants and their (bio)transformation products in toxicology: polychlorinated biphenyls as an example. Environ Sci Pollut Res Int 25(17):1-14. doi:10.1007/s11356-017-1162-0 PMID:29322390 PMCID:PMC6015536
to Top