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University of Iowa: Dataset Details, ID=doi: 10.6084/m9.figshare.8269832.v1

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Superfund Research Program

Airborne PCBs: Sources, Exposures, Toxicities, Remediation

Center Director: Keri C. Hornbuckle
Grant Number: P42ES013661
Funding Period: 2006-2025
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Title: Authentication of 3,3'-dichloro-4,5-dimethoxy-biphenyl

Accession Number: doi: 10.6084/m9.figshare.8269832.v1

Link to Dataset: https://figshare.com/articles/Authentication_of_3_3_-dichloro-4_5-dimethoxy-biphenyl/8269832/1

Repository: figshare

Data Type(s): Chemical & Chemical Biology

Summary: 3,3'-Dichloro-4,5-dimethoxy-biphenyl is a derivative of PCB 11 (3,3'-dichlorobiphenyl) and was synthesized as an analytical standard to study the metabolism of PCB 11, a polychlorinated biphenyl (PCB) congener that is not present in technical PCB mixtures. This compound was synthesized via Suzuki cross coupling of 5-bromo-3-chloro-1,2-dimethoybenzene and 3-chlorophenylboronic acid.

Publication(s) associated with this dataset:
  • Li X, Holland EB, Feng W, Zheng J, Dong Y, Pessah IN, Duffel MW, Robertson LW, Lehmler H. 2018. Authentication of synthetic environmental contaminants and their (bio)transformation products in toxicology: polychlorinated biphenyls as an example. Environ Sci Pollut Res Int 25(17):1-14. doi:10.1007/s11356-017-1162-0 PMID:29322390 PMCID:PMC6015536
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