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Your Environment. Your Health.

Project Publications: University of Cincinnati: Chromatography/Plasma MS for Ultra-trace Analysis

Superfund Research Program

Chromatography/Plasma MS for Ultra-trace Analysis

Project Leader: Joseph A. Caruso
Grant Number: P42ES004908
Funding Period: 1995 - 2001

Project-Specific Links

Publications

2008

  • Ellis J, Grimm R, Clark JF, Wilbur S, Caruso JA. 2008. Studying protein phosphorylation in low MW CSF fractions with capLC-ICPMS and nanoLC-CHIP-ITMS for identification of phosphoproteins. J Proteome Res 7(11):4736-4742. doi:10.1021/pr800294r PMID:18808172 PMCID:PMC2765409

2000

  • Brisbin JA, Sutton KL, Caruso JA, B'Hymer C. 2000. New approaches for elemental speciation using plasma mass spectrometry. American Laboratory 32(3):17-23.
  • Day JA, Caruso JA, B'Hymer C. 2000. Evaluation of a microconcentric nebulizer and its suction effect in a capillary electrophoresis interface with inductively coupled plasma-mass spectrometry. Applied Spectroscopy 54(7):1040-1046.
  • Day JA, Sutton KL, Soman RS, Caruso JA. 2000. A comparison of capillary electrophoresis using indirect UV absorbance and ICP-MS detection with a self-aspirating nebulizer interface. Analyst 125(5):819-823.
  • Milstein LS. 2000. A mixed gas helium/argon low power/reduced-pressure ICP as tunable ionization sources for the mass spectrometric detection of organotin compounds. Applied Spectroscopy 54(9):1286-1290.
  • Ponce de Leone C, Sutton KL, Caruso JA, Uden P. 2000. Chiral speciation of selenoamino acids and selenium enriched samples using HPLC coupled to ICP-MS. J Anal At Spectrom 15(9):1103-1107.
  • Sutton KL, Ponce de Leone C, Ackley KL, Sutton RM, Stalcup AM, Caruso JA. 2000. Development of chiral HPLC for selenoamino acids with ICP-MS detection:application to selenium nutritional supplements. Analyst 125(2):281-286. PMID:10866603
  • Waggoner JW, Milstein LS, Belkin M, Sutton KL, Caruso JA. 2000. Application of a novel low power/reduced pressure helium ICP ionization source for mass spectrometric detection of organobromine compounds and derivatized organotin compounds. J Anal At Spectrom 15:13-19.

1999

  • Ackley KL, Day JA, Sutton KL, Caruso JA. 1999. Investigation of problems associated with the determination of iodine in glacial acetic acid samples using flow injection analysis-inductively coupled plasma-mass spectrometry. Analytical Communications 36:295-299.
  • Ackley KL, Sutton KL, Caruso JA. 1999. Speciation of arsenic in fish tissue using microwave assisted extraction followed by HPLC-ICP-MS. J Anal At Spectrom 14:845-850.
  • Gbatu TP, Ceylan O, Sutton KL, Rubinson JF, Galal A, Caruso JA, Mark HB. 1999. Electrochemical control of solid phase micro-extraction using unique conducting polymer coated fibers. Analytical Communications 36:203-205.
  • Gbatu TP, Sutton KL, Caruso JA. 1999. Preparation and characterization of hydrophobic coatings by sol-gel technology for SPME-HPLC determination of organometals. Anal Chim Acta 402:67-79.
  • Sutton KL, Caruso JA, B'Hymer C. 1999. The use of sol-gel frits to minimize suction effects in capillary electrophoresis-nebulizer interfaces for plasma spectrometry. Analytical Communications 36:349-352.

1998

  • Belkin M, Caruso JA. 1998. Qualitative analysis of nonconducting oxide-based materials with radio frequency glow discharge mass spectrometry. Canadian Journal of Analytical Sciences and Spectroscopy 43:8-13.
  • Belkin M, Caruso JA, Christopher SJ, Marcus RK. 1998. Characterization of helium/argon working gas systems in a radiofrequency glow discharge atomic emission source. Part II: Langmuir probe and emission intensity studies for Al, Cu and Macor samples. Spectrochimica Acta Part B: Atomic Spectroscopy 53:1197-1208.
  • Caruso JA, Vela NP, Olson LK. 1998. New Departures for Elemental Speciation Studies Utilizing Plasma Mass Spectrometric Detection. Chapter 8. In: Metals in Surface Waters. Ann Arbor Press, Ann Arbor, MI. pp.155-166.
  • Christopher SJ, Marcus RK, Belkin M, Caruso JA. 1998. Characterization of helium/argon working gas systems in a radiofrequency glow discharge atomic emission source. Part I: Optical emission, sputtering, and electrical characteristics. Spectrochimica Acta Part B: Atomic Spectroscopy 53:1181-1196.
  • Kirlew PW, Caruso JA. 1998. Investigation of a modified oscillating capillary nebulizer design as an interface for CE-ICP-MS. Applied Spectroscopy 52:770-772.
  • Kirlew PW, Castillano MT, Caruso JA. 1998. A comparison of ultrasonic nebulizers as interfaces for capillary electrophoresis of inorganic anions and cations with ICP-MS detection. Spectrochim Acta A Mol Biomol Spectrosc 53:221-237.
  • Montaser A, Minnich MG, McLean JA, Liu H, McLeod CW, Caruso JA. 1998. Sample Introduction in ICPMS. In: Inductively Coupled Plasma Mass Spectrometry. Wiley-VCH, NY.
  • Sutton KL, Caruso JA, B'Hymer C. 1998. A comparison of UV absorbance and inductively coupled plasma mass spectrometry detection for capillary electrophoresis. J Anal At Spectrom 13:885-891.
  • Sutton KL, Caruso JA, B'Hymer C. 1998. A comparison of four nebulizer/spray chamber interfaces for the high performance liquid chromatographic separation of arsenic compounds using ICP-MS detection. J Anal At Spectrom 13:855-858.
  • Tomlinson MJ, Caruso JA. 1998. Coupled Instrumentation Methods (Plasma Mass Spectrometry)/Sample Introduction. In: Encyclopedia of Scientific Instrumentation. American Chemical Society,
  • Zhang H, Montaser A, Zimmer H, Vela NP, Caruso JA. 1998. Mass Spectrometry with Microwave-Induced Plasmas. In: Inductively Coupled Plasma Mass Spectrometry. Wiley-VCH, NY. pp.891-939.
  • Zoorob G, McKiernan J, Caruso JA. 1998. Chromatography/plasma mass spectrometry for elemental speciation studies. Microchimica Acta 128(3-4):145-168.

1997

  • Belkin M, Caruso JA. 1997. Radio frequency glow discharge as an ion source for gas chromatography with mass spectroscopic detection. J Anal At Spectrom 12:1255-1260.
  • Castillano MT, Giglio JJ, Evans EH, Caruso JA. 1997. Solution nebulization into a low-pressure helium inductively coupled plasma with mass spectrometric detection. J Anal At Spectrom 12:383-385.
  • Gorecki T, Belkin M, Caruso JA, Pawliszyn J. 1997. Solid phase microextraction as sample introduction technique for radio frequency glow discharge mass spectrometry. Analytical Communications 34:275-277.
  • Sutton RM, Sutton KL, Caruso JA. 1997. ICP-MS detection for chromatography and capillary electrophoresis: a review. J Chromatogr A 789:85-126.
  • Vela NP, Satzger RD, Caruso JA. 1997. Potential for an atmospheric pressure low-power microwave induced plasma ionization source for mass spectrometry. Applied Spectroscopy 51:1500-1503.
  • Zoorob G, Byrdy FB, Caruso JA. 1997. Electrospray mass spectrometry as a technique for the elemental analysis of metals and organometals. J Anal At Spectrom 12:517-524.
  • Zoorob G, Caruso JA. 1997. Speciation of chromium dyes by high performance liquid chromatography with inductively coupled plasma mass spectrometric detection. J Chromatogr A 773:157-162. PMID:9228796

1996

  • Byrdy FB, Olson LK, Caruso JA. 1996. Comparison of electrospray and inductively coupled plasma sources for elemental analysis with mass spectrometric detection. J Anal At Spectrom 11:633-641.
  • Ding H, Olson LK, Caruso JA. 1996. Elemental speciation for chromium in chromium picolinate products. Spectrochimica Acta Part B: Atomic Spectroscopy 51(B):1801-1812.
  • O'Connor G, Ebdon L, Evans EH, Ding H, Olson LK, Caruso JA. 1996. Feasibility study of low pressure inductively coupled plasma mass spectrometry for qualitative and quantitative speciation. J Anal At Spectrom 11:491-496.
  • Olson LK, Belkin M, Caruso JA. 1996. Radiofrequency glow discharge mass spectrometry for gas chromatographic detection: a new departure for elemental speciation studies. J Anal At Spectrom 11:491-496.
  • Tomlinson MJ, Caruso JA. 1996. Speciation of chromium using thermospray nebulization as sample introduction into ICP-MS. Anal Chim Acta 322:1-9.
  • Vela NP, Caruso JA. 1996. Trace metal speciation via SFE-LC-ICP-MS. J Anal At Spectrom 11:1129-1135.

1995

  • Byrdy FB, Caruso JA. 1995. Selective Chromatographic Detection by Plasma Mass Spectrometry. In: Selective Detectors for Chemical Analysis. Chemical Analysis Series. John Wiley & Sons, New York, NY. pp.171-207.
  • Byrdy FB, Caruso JA. 1995. Trace metal speciation by HPLC with plasma source MS detection. Environ Health Perspect 103(Suppl.1):21-23. PMID:7621792
  • Byrdy FB, Olson LK, Vela NP, Caruso JA. 1995. Chromium speciation by anion-exchange high-performance liquid chromatography with both inductively coupled plasma atomic emission spectroscopic and inductively coupled plasma mass spectrometric detection. J Chromatogr A 712(2):311-320. doi:10.1016/0021-9673(95)00528-U PMID:7581851
  • Cleland TJ, Bonchin-Cleland S, Olson LK, Meeks FR, Caruso JA. 1995. More efficient ion transport for inductively coupled plasma mass spectrometry. Spectrochimica Acta Part B: Atomic Spectroscopy 50(B):873-884.
  • Ding H, Wang J, Dorsey JG, Caruso JA. 1995. Arsenic speciation by micellar liquid chromatography with ICP-MS detection. J Chromatogr A 694(2):425-431. PMID:7535627
  • Giglio JJ, Caruso JA. 1995. Evaluation of alternate plasma gases for rf glow discharge mass spectrometry. Applied Spectroscopy 49:900-906.
  • Giglio JJ, Caruso JA. 1995. Evaluation of direct injection nebulizer for liquid sample introduction in helium microwave induced plasma mass spectrometry. Applied Spectroscopy 49:314-319.
  • Kumar UT, Vela NP, Caruso JA. 1995. Multi-element detection of organometals by supercritical fluid chromatography with ICP-MS detection. Journal of Chromatographic Science 33(11):606-610. PMID:7593407
  • Lin L, Wang J, Caruso JA. 1995. Arsenic speciation using capillary zone electrophoresis with indirect UV detection. Journal of Chromatographic Science 33(4):177-180.
  • Marawi I, Olson LK, Wang J, Caruso JA. 1995. Utilization of metallic platforms in electrothermal vaporization ICP-MS. J Anal At Spectrom 10:7-14.
  • Olson LK, Vela NP, Caruso JA. 1995. Hydride generation, electrochemical vaporization and liquid chromatography as sample introduction techniques for ICP-MS. Spectrochim Acta A Mol Biomol Spectrosc 50(B):355-368.
  • Tomlinson MJ, Lin L, Caruso JA. 1995. Plasma mass spectrometry as a detector for chemical speciation studies. Analyst 120(3):583-589. PMID:7741220
  • Wang J, Tomlinson MJ, Caruso JA. 1995. Extraction of trace elements in coal fly ash and subsequent speciation by high-performance liquid chromatography with ICP-MS. J Anal At Spectrom 10:601-607.
  • Ziegler JW, Dorsey JG, Chester TL, Innis DP. 1995. Estimation of liquid-vapor critical loci for CO2-solvent mixtures using a peak-shape method. Anal Chem 67(2):456-461. PMID:7856887
  • Zoorob G, Tomlinson MJ, Wang J, Caruso JA. 1995. Evaluation of the direct injection nebulizer in the coupling of HPLC to ICP-MS. J Anal At Spectrom 10:853-858.

1994

  • Carey JM, Vela NP, Caruso JA. 1994. Chromium determination by supercritical fluid chromatography with inductively coupled plasma mass spectrometric and flame ionization detection. J Chromatogr A 662(2):329-340. PMID:8143029
  • Kumar UT, Dorsey JG, Caruso JA, Evans EH. 1994. Metalloporphyrin speciation by liquid chromatography and inductively coupled plasma-mass spectrometry. Journal of Chromatographic Science 33(7):282-285. PMID:8063886

1993

  • Kumar UT, Vela NP, Dorsey JG, Caruso JA. 1993. Supercritical fluid extraction of organotins from biological samples and speciation by liquid chromatography and inductively coupled plasma mass spectrometry. J Chromatogr A 655(2):340-345. PMID:8111474

1992

  • Dorsey JG, Foley JP, Cooper WT, Barford RA, Barth HG. 1992. Liquid chromatography: theory and methodology. Anal Chem 64(12):353R-389R. doi:10.1021/ac00036a020 PMID:1626705
  • Sheppard BS, Caruso JA, Heitkemper DT, Wolnik KA. 1992. Arsenic speciation by ion chromatography with inductively coupled plasma mass spectrometric detection. Analyst 117(6):971-975. PMID:1503234
  • Story WC, Caruso JA, Heitkemper DT, Perkins L. 1992. Elimination of the chloride interference on the determination of arsenic using hydride generation inductively coupled plasma mass spectrometry. Journal of Chromatographic Science 30(11):427-432. PMID:1474130

1991

  • Shen W, Vela NP, Sheppard BS, Caruso JA. 1991. Evaluation of inductively coupled plasma mass spectrometry as an elemental detector for supercritical fluid chromatography. Anal Chem 63(14):14911496. PMID:1928724

1990

  • Heitkemper DT, Creed J, Caruso JA. 1990. Helium microwave-induced plasma mass spectrometric detection for reversed-phase high-performance liquid chromatography. Journal of Chromatographic Science 28(4):175-181. PMID:2079547
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