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National Institute of Environmental Health Sciences

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Your Environment. Your Health.

University of Iowa: Dataset Details, ID=doi:10.6084/m9.figshare.10299302.v1.

Superfund Research Program

Research Support Core: Synthesis Core

Project Leader: Hans-Joachim Lehmler
Co-Investigator: Xueshu Li
Grant Number: P42ES013661
Funding Period: 2006-2025
View this project in the NIH Research Portfolio Online Reporting Tools (RePORT)

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Title: Authentication of 4-chloro-3-hydroxy-biphenyl

Accession Number: doi:10.6084/m9.figshare.10299302.v1.

Link to Dataset: https://figshare.com/articles/Authentication_of_4-chloro-3-hydroxy-biphenyl/10299302

Repository: figshare

Data Type(s): Chemical & Chemical Biology

Summary: Authentication of 4-chloro-3-hydroxy-biphenyl by 1H NMR, 13C NMR, and GC-MS. The title compound was synthesized by demethylation of 3-methoxy-4-chloro-biphenyl in the presence of BBr3. The purity (>99 ) of the compound was determined based on relative peak area by GC-MS. Keyword(s) authentication environmental pollutants metabolite Organic Compounds PCBs PCB 3 polychlorinated biphenyls Superfund chemicals

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